
What is 3D X-Ray Microscopy?
Application Examples

Capabilities beyond microCT
A new field of 3D X-ray microscopy (XRM) has emerged, bringing dramatic resolution and contrast improvements to X-ray tomographic imaging. It offers more than traditional X-ray microCT for a variety of applications.
- Materials Characterization: Composites
- Microstructural Evolution: Metals
- Process Development: Additive Manufacturing
- Failure Analysis: Electronics

Composite sample imaged at 0.8 micron voxel. Sample courtesy of Professor Milani, University of British Columbia
Materials Characterization: Composites
- The superior contrast and resolution of XRM facilitates easier separation of low Z materials at sub-micron resolution
- Quantitative information such as void content, fiber orientation, and fiber distribution is easily determined
- Complex composite image is segmented to a 3D dataset of glass fibers (green), polypropylene fibers (orange), and voids (white)

Steel sample imaged at 1.5 micron voxel. Sample provided by Sandia National Laboratories
Microstructural Evolution: Metals
- 3D in situ imaging requires samples inside larger load stage. XRM's unique detector design allows for large working distances while maintaining "Resolution at a Distance" (RaaD)
- RaaD allows you to non-destructively characterize and quantify the evolution of 3D microstructures with high resolution
- Images show in situ tensile testing of a laser welded steel sample under increasing load. The data reveals a crack initiating from rough surface imperfections (top), as well as the elongation of internal voids (bottom)
Aluminum additive manufacturing part images at 20 micron full field of view and 3 micron ROI. Sample courtesy of Aalen University
Process Development: Additive Manufacturing
- XRM allows you to choose an interior sample region for interior tomography while keeping samples intact
- Unlike microCT, with unique detector design you can select your magnification and field-of-view to optimize resolution - just like in a microscope!
- XRM scans can measure porosity with sub-micron resolution and be used for 3D printing files (STL)
Intact 50 mm 2.5 interposer sample imaged at 14.5 μm and 1 μm voxel resolution
Failure Analysis: Electronics
- Video shows non-destructive imaging of an electronics package with 2.5D interposer after thermal cycling. Internal defects in C4 and micro-bumps are clearly visualized
- "Resolution-at-a-Distance" (RaaD) allows region of interest imaging at high resolution (<1 micron voxel resolution) with no sample trimming
- This technique allows observation of failure evolution during progressive testing in many devices, as well as general non-destructive investigation of packaging failures of all types
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