advanced microscopy techniques

Designing Lighter, Faster, and Stronger Engineering Materials

By revealing complex processing-structure-property relationships
Engineering the Future of Materials Science Whether designing new metals and alloys, composites, ceramics, or cementitious materials, characterization techniques play a critical role in establishing the process-structure-property relationships that define these materials’ performance. Explore the latest microscopy methods from ZEISS, and how they are helping researchers better understand their materials across lengthscales, through dimensions, and under stimulus.
  • Multiscale Characterization

    Connect your sample and image data seamlessly across different length scales and microscopes.

  • Microstructures in 3D

    Understand how complex 3D microstructure and morphology impact material properties.

  • In Situ Material Dynamics

    Observe real-time behavior under thermal or mechanical load.

Microstructural Imaging in the Metals R&D Lab
  • Liberty University has a relatively new and small engineering program… a lot of this [characterization equipment] is new to the university. It’s something we’re incorporating more and moreinto the curriculum.​ So when I’m thinking in terms of how to apply in situ testing, I’m often looking at a reality where most of the students are probably new to SEM in general – and then on top of that needing to learn in situ testing is really important but also [needs to be] manageable.

    Prof. Mark Atwater Liberty University
  • We employed LabDCT – laboratory diffraction contrast tomography. It’s a 3D nondestructive technique, which allows us to really capture the full picture of the microstructure. And by being nondestructive, we can also track microstructural evolution through time steps [of grain coarsening] … and try to figure out what triggers abnormal grain growth.

    Yi Wang PhD Candidate, Carnegie Mellon University
  • Across many grains and many indents, I can now observe [with controlled ECCI on a ZEISS SEM] each of these indents with their dislocation structures around them, and in this way obtain much better statistics than from a single experiment. So I can separate what is really systematic behavior of dislocations and what is stochastic behavior. Furthermore, I can investigate effects across different grain orientations or proximity to grain boundaries.

    Prof. Stefan Zaefferer Max Planck Institute
  • Optical inspection is very fast, and you can quickly go through your sample and identify regions of interest. Then when the sample comes to the electron microscope, perhaps even with a different operator, they don’t need to use some convoluted map or disjointed or manually annotated images but rather can navigate directly in the ZEN Connect environment to find the regions of interest and drive directly to them with the SEM.

    Nathaniel Cohan ZEISS Applications Engineer

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What types of microscopy techniques are available for research of engineering materials?

ZEISS offers a variety of microscopy techniques tailored for materials design and engineering including:
  • ZEISS offers a variety of microscopy techniques tailored for materials design and engineering including:
    • Optical Microscopy: Addresses all typical metallography tasks using upright, inverted, zoom, digital, and confocal systems. Perform analysis of grain size, non-metallic inclusions, cast iron graphite, alloy multi-phase distributions, coating or layer thickness, surface roughness, or technical cleanliness.
    • Electron Microscopy: Provides ultra-high resolution for nanoscale visualization of material surfaces. Reveal precipitate phases, grain microstructures, crystal lattice defects and dislocations, chemical mapping, or perform automated in situ loading experiments.
    • FIB-SEM Microscopy: Extends SEM analysis to the sub-surface with the addition of a gallium focused ion beam for targeted milling. Enables microscale sample preparation of pillars, dogbones, or TEM lamella, and also facilitates serial sectioning 3D tomography. By combining FIB-SEM with a femtosecond (fs) laser, researchers cover a huge range of material ablation demands.
    • 3D X-ray Microscopy: Delivers nondestructive 3D imaging by high resolution X-ray tomography. Perfect for analysis of internal sample features or morphology like voids, cracks, distributed particles, or crystalline microstructures.
    These systems come together to form a versatile portfolio, empowering you to investigate the diverse range of features that exist within modern engineering materials.
  • The ZEISS microscopy portfolio is designed to address four key types of characterization challenges often faced by materials scientists:

    • Routine Metallography: Fundamental characterization of metallic microstructures requires routine, efficient analysis of characteristics like grain sizes, phase distributions, and inclusion analysis. The different light microscope configurations from ZEISS, in combination with ZEN Core acquisition and analysis software, makes sure a researcher can perform these tasks easily, and in accordance with industry standards.
    • Multiscale Imaging: Many engineering materials display hierarchical structures, with critical features spanning from the macro- to nano-scales. The extensive optical, electron, and X-ray portfolio of microscopes from ZEISS is designed not only to cover this range of needs, but help researchers connect their samples and image data to navigate through the different lengthscales and instruments in a coordinated and intelligent manner.
    • 3D Characterization: The complex structures found in engineering materials usually exist in three dimensions, therefore it can be critical to work with imaging techniques that reflect and capture that complexity. ZEISS offers confocal laser scanning microscopy, 3D X-ray microscopy, and FIB-SEM tomography techniques to ensure materials’ structures are visible in all three spatial dimensions.
    • In Situ Experiments: To best understand how a material will perform in a given application, scientists are often interested in observing how microstructures react under real operational conditions or under imposed stimulus/load. The ZEISS microscopy portfolio offers a variety of in situ experimental rigs and stages to easily facilitate such workflows.
  • The ZEISS microscopy portfolio addresses imaging needs across a broad range of material types:

    • Metals & Alloys: ZEISS microscopes address the full range of characterization needs for metals and alloys research, from routine metallography to advanced 3D and in situ characterization.
    • Composites: Composites, particularly fiber-reinforced polymer composites, are compelling alternatives to metallic materials, especially in weight-sensitive applications. X-ray microscopes from ZEISS, such as the VersaXRM, provide 3D images of fiber and matrix distributions that can be critical to understanding the unique, and sometimes highly anisotropic, 3D structures often found in these materials.
    • Ceramics: ZEISS scanning electron microscopes, often in combination with focused ion beam, provide high resolution and surface sensitive imaging that is ideally suited to nano- and micro-scale features and grain sizes often seen in ceramic materials.
    • Cementitious Building Materials: Concretes and similar building materials are critical for their high strength and low cost. Advanced imaging, such as with ZEISS 3D X-ray microscopy, can help better understand the connections between structure and mechanical properties, or even lead to advances in growing fields like self-healing materials.